By Leonard, John; Lygo, B.; Procter, Garry
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These specifications are typically published on the journal publisher’s website. Once you have decided which specification to comply with, make sure that you collect an adequate range of data for all your compounds as you prepare them. It will also save you many hours of work if you compile data in the format you have chosen from the outset of your work. For most purposes, the data specified as follows will normally be required for characterization purposes: 1. Crystalline solid characteristics For solids, the melting point should be specified, together with the solvent from which the compound was crystallized.
3. The Experimental Section This section contains the method(s) of preparation for each compound, together with a set of data that is adequate to characterize it. The range of data presented and the style of presentation must conform to strict technical requirements, and it is most important that the appropriate standards are understood and adhered to. 2 Planning a report or thesis Planning is the key to writing a good report or thesis. From the outset, you should aim to construct the document so that it has a logical structure and is easy to follow.
Chapter three: Keeping records of laboratory work 17 Flash chromatography using 9:1 (pet. 1 An example of a laboratory notebook entry. 4 Paper laboratory notebook: Suggested laboratory notebook format 1. General layout It is good practice to start each new experiment on the next free right-hand page of the laboratory book. This makes finding any particular experiment easier. 2. Experiment number Every experiment should be assigned a unique reference number. This number is usually placed in the top right-hand corner of the laboratory book page.
Advanced practical organic chemistry by Leonard, John; Lygo, B.; Procter, Garry